Measurement Example of Environmentally Restricted Substances

Measurement of Solder Samples

SEA1200VX achieves highly sensitive results by measuring Pb-free solder samples at providing superior “limit of detection” and excellent repeatability.

[ Lead (Pb) in Pb Free Solder by SEA1200VX ]

Excellent linearity of the calibration curve for Pb-free solder created by optimal measurement conditions achieves a detection lower limit of 7.9ppm Pb at a measuring time of 300 seconds.
Pb in Pb Free Solder
Pb in Pb Free Solder
DL at 300 Meas. Time: 7.9ppm

[ Excellent Repeatability ]

SEA1200VX achieves a significantly higher repeatability of CV 1.9 % at a measuring time of 100 seconds using an MBH Pb-free solder standard sample.

 
< Measurement Conditions >
Voltage : 40kV
Current : 1000µA
Collimator : φ8mm
Filter : for Pb
Meas. Time : 100 sec.

< Standard Sample >
MBH 74X HA

Ave. (ppm)

590
Readings
20
STDEV (ppm)
11.3
CV%
1.9
Conc. (ppm)
615

[ Application to Real Samples ]

The following tables and graph show an example of a Pb-free solder measurement by SEA1200VX achieving better correlation with ICP-OES.

  < Measurement Conditions >
Voltage : 40kV
Current : 1000µA
Collimator : φ8mm
Filter : for Pb
Time : 300 sec.
Application to Real Sample
Spectrum of Sample 3
  < Comparison with ICP-OES and XRF data >
Sample
ICP-OES
XRF
1
310
310
2
308
299
3
42.1
45.0
4
113
120
(unit : ppm)


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